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Fig. 5. (a)Micrographs of the specimens treated at 16001C for 2, 4, and

8 h. (b) Conductivity profiles by two-microelectrode measurements as a

function of the normalized distance with respect to the thickness of the

large-grained nitrided layers. (c) Conductivity profiles by one-microelectrode

measurements as a function of the normalized distance.

Fig. 6. Impedance spectra of tetragonal zirconia polycrystal (TZP) region

of the specimen nitrided at 16001C for 2 h (Fig. 5) using two microelectrodes

(a), using one microelectrode at different positions (b, c)

(versus the counterelectrode), while (d) shows a spectrum of the pristine

2 mol% yttria-doped tetragonal zirconia polycrystals (2Y-TZP) ceramics

using macro-sized electrodes.